Method for treating waste material

Abstract

Preheated diluent and steam are introduced into a container containing waste material typically comprised of a sludge mixture of liquid and solid material including hydrocarbons. The material is thereby heated and its viscosity reduced to form a pumpable slurry. The slurry is pumped out of the container and its viscosity is adjusted to the optimum for separating the solids and liquids. The solids are then separated from the liquid, any valuable material in either the solids and the liquid are recovered and the rest disposed of.

What is claimed is: . .1. A method for removing waste material having solid and liquid phase components from a container and separating said components, comprising: 
     
        central location within said container..!.. .10.  The method of claim 1 wherein said step of injecting a first quantity of said steam is at a plurality of locations disposed radially outwards of and about said central location and within said container..!.. .11. The method of claim 10 wherein said waste material includes at least one hydrocarbon; and wherein said diluent is heated to a temperature no higher than about twenty degrees Fahrenheit less than the flash point of the hydrocarbon in said at least one hydrocarbon having the lowest flash point..!.. .12. A method of removing and separating liquid hydrocarbons and solids that have settled as sludge to the bottom of a container comprising injecting liquid diluent in which the hydrocarbons are soluble into the container and heating the sludge to convert the sludge into a pumpable slurry of diluted liquids and suspended solids, pumping the slurry out of the tank, adding heat as required to adjust the viscosity of the slurry for separation of the solids from the liquids in the slurry, and separating the solids from the liquid..!.. .13. The method of claim 12 in which adding heat includes adding additional heated diluent..!.. .14. The method of claim 12 in which the diluent is heated to a temperature just below the lowest flash point temperature of the material making up the sludge or the flash point of the diluent, whichever is the lower..!.. .15. The method of claim 12 in which the solids are separated from the liquid by centrifugal 
     
     
        force..!..Iadd.     A method for removing waste material having solid and liquid phase components from a container and separating said components, comprising: heating a diluent; injecting a first quantity of steam and said diluent into said container directly against said waste material in an amount sufficient to cause a portion of said solid phase to flow; establishing a flow of a portion of said liquid phase and said portion of said solid phase of said waste material from said container; injecting a second quantity of steam and said diluent into said flow of waste material in an amount sufficient to maintain said flow; injecting a third quantity of said steam and said diluent into said flow of waste material injected with said second quantity of said steam and diluent, said steam and diluent being in an amount functionally related to said waste material in said container to optimize said separating of said liquid and solid phases; separating said liquid and said solid phases of said waste material from said flow of said waste material by centrifugal force; and collecting volumes of said liquid and said solid phases of said waste material from said separated liquid and solid phases..Iaddend..Iadd.17. A method of removing and separating liquid hydrocarbons and solids that have settled as sludge to the bottom of a container comprising injecting liquid diluent in which the hydrocarbons are soluble into the container and heating the sludge to convert the sludge into a pumpable slurry of diluted liquids and suspended solids, pumping the slurry out of the tank, adding steam as required to adjust the viscosity of the slurry for separation of the solids from the liquids in the slurry, and separating the solids from 
     
     
        the liquid by centrifugal force..Iaddend..Iadd.18.  A method of removing sludge from a tank containing fine solid particles of catalyst and hydrocarbons comprising introducing a diluent and heating the sludge so as to create a pumpable slurry, pumping the slurry out of the tank, maintaining the desired viscosity of the slurry with further diluent and heating, and separating the solids from the liquids in the slurry by use of a centrifuge while injecting live steam into the slurry between the feed pump to the centrifuge and the centrifuge..Iaddend.