Antibacterial product

Abstract

A number of water-soluble, one-to-one quaternary ammonium adducts of unsaturated organic halides and dihalides with hexamethylenetetramine are known as being useful as antimicrobial agents. It has now been discovered that a two-to-one quaternary ammonium adduct can be prepared from hexamethylenetetramine and 3,4-dichlorobutene-1; this two-to-one adduct is a more active, less toxic antimicrobial agent than the known one-to-one quaternary ammonium adducts.

We claim: 
     
       1. A method for preparing the two-to-one quaternary ammonium adduct of hexamethylenetetramine and 3,4-dichlorobutene-1 which comprises reacting 3,4-dichlorobutene-1 with hexamethylenetetramine at a temperature of less than about 130° C. in an inert organic solvent in which the adduct is substantially insoluble, .Iadd.said adduct having antibacterial activity and having the structural formula: ##STR2##  .[. 
     
     
       2.  A composition consisting essentially of the two-to-one quaternary ammonium adduct of hexamethylenetetramine and 3,4-dichlorobutene-1..].