US7674410B2ExpiredUtilityA1

Method for manufacturing a thermal interface material

Assignee: UNIV TSINGHUAPriority: Apr 14, 2005Filed: Dec 29, 2005Granted: Mar 9, 2010
Est. expiryApr 14, 2025(expired)· nominal 20-yr term from priority
H10W 40/73H10W 40/25B81C 1/0069Y10S977/88Y10S977/753Y10S977/789Y10S977/842Y10S977/84
92
PatentIndex Score
31
Cited by
24
References
15
Claims

Abstract

A method for manufacturing a thermal interface material comprising the steps of: providing a carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends; forming a composite phase change material by filling clearances in the carbon nanotube array with a phase change material; forming a section with predetermined thickness by cutting the composite phase change material along a direction cross to an alignment direction of the carbon nanotubes; and heating up the section to a temperature higher than a phase change temperature of the phase change material and cooling down after the two opposite ends of the carbon nanotubes protruding out of the section.

Claims

exact text as granted — not AI-modified
1. A method for manufacturing a thermal interface material comprising the steps of:
 providing a carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends; 
 forming a composite phase change material by filling clearances in the carbon nanotube array with a paraffin; 
 cutting the composite phase change material to form a section and bending the ends of the carbon nanotubes, wherein the cutting of the composite phase change material is done along a direction that is at an angle to an alignment direction of the carbon nanotubes and bends the ends of the carbon nanotubes; and 
 heating the section to a temperature of 60 degrees Celsius until the ends of the carbon nanotubes become unbent and protrude out of the section. 
 
   
   
     2. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein the step of forming the composite phase change material comprising steps of:
 immersing the carbon nanotube array into xylene; 
 putting paraffin into the xylene at 60 degrees Celsius; 
 evaporating the xylene; and 
 cooling the paraffin down. 
 
   
   
     3. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein the carbon nanotubes are formed by a chemical vapor deposition method or a deposition method. 
   
   
     4. The method for manufacturing a thermal interface material in accordance with  claim 3 , wherein a catalyst used in the chemical vapor deposition method is made from a material selected from the group comprising of iron, cobalt, nickel, and palladium. 
   
   
     5. The method for manufacturing a thermal interface material in accordance with  claim 3 , wherein a carbon source gas used in the chemical vapor deposition method is selected from the group comprising of methane, ethylene, propylene, acetylene, methanol, and ethanol. 
   
   
     6. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein the carbon nanotubes are substantially parallel to each other. 
   
   
     7. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein a thickness of the section is in a range from about 1 μm to about 100 μm. 
   
   
     8. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is in a range from about 0.2% to about 10% by volume. 
   
   
     9. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is about 10% by volume. 
   
   
     10. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is about 0.2% by volume. 
   
   
     11. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein the angle is approximately ninety degrees. 
   
   
     12. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein after cutting the composite phase change material, the carbon nanotubes in the section are in the shape of a “U”. 
   
   
     13. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein after cutting the composite phase change material, the carbon nanotubes in the section are formed in the shape of a “Z”. 
   
   
     14. The method for manufacturing a thermal interface material in accordance with  claim 1 , wherein bending directions of the ends of the carbon nanotubes varies according to the direction of the cutting of the composite phase change material. 
   
   
     15. A method for manufacturing a thermal interface material comprising the steps of:
 providing a composite phase change material comprising of carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends and a paraffin filling clearances within the carbon nanotube array; 
 cutting the composite phase change material to form a section and bending the ends of the carbon nanotubes, wherein the cutting of the composite phase change material bends the ends of the carbon nanotubes and is done along a direction that is at an angle to an alignment direction of the carbon nanotubes; and 
 heating the section until the ends of the carbon nanotubes become unbent and protrude out of the section.

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