US2025230583A1PendingUtilityA1
Process for preparing a carbon fiber precursor
Individually held — no corporate assignee on recordPriority: Apr 24, 2023Filed: Apr 1, 2025Published: Jul 17, 2025
Est. expiryApr 24, 2043(~16.7 yrs left)· nominal 20-yr term from priority
Inventors:Leander Francis Aulisio
D01D 13/00D10B 2101/12D01D 1/02D01D 10/02D10B 2321/10D01F 9/328D01F 6/18D01F 9/22D01F 9/225
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Claims
Abstract
A process for preparing a carbon fiber precursor is hereby disclosed, wherein the precursor is selected from a series of solid PAN (polyacrylonitrile) fibers, wherein each member of the series contains about 0.5 mole % to about 8 mole % ammonium salt of 2-acrylamido-2-methyl propane sulfonic acid.
Claims
exact text as granted — not AI-modified1 . A process for preparing a carbon fiber precursor, the process comprising:
(a) obtaining a series of monomer mixtures, wherein each mixture of monomers comprises acrylonitrile and an ammonium salt of 2-acrylamido-2-methyl propane sulfonic acid; (b) individually polymerizing the monomer mixtures to obtain a PAN polymer; (c) individually spinning the PAN polymer to obtain PAN filaments; (d) individually bundling the filaments to obtain a PAN fiber; (e) individually analyzing the PAN fiber for a physical property, wherein the property is a member selected from the group consisting of: number of surface defects, interior homogeneity, degree of orientation, tenacity, number and size of micro voids, arrangement of crystallites on the surface, compactness of structure, and combinations thereof; and (f) ranking the PAN fiber, wherein a most highly ranked solid PAN fiber is the carbon fiber precursor.
2 . The process according to claim 1 wherein the acrylonitrile monomer is present in an amount of about 92 mole % to about 99.5 mole %, and the ammonium salt of 2-acrylamido-2-methyl propane sulfonic acid monomer is present in an amount of about 0.5 mole % to about 8 mole %.
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