US2019167820A1PendingUtilityA1

Novel aryl ethene derivative and pharmaceutical composition containing same as active ingredient

Assignee: HWANG SUNG YEOUNPriority: Jun 27, 2016Filed: Sep 13, 2016Published: Jun 6, 2019
Est. expiryJun 27, 2036(~9.9 yrs left)· nominal 20-yr term from priority
A61K 31/454A61K 31/407C07D 241/04C07D 203/08A61K 31/5375A61K 31/403A61K 31/496A61K 31/495A61K 31/396A61K 31/40A61K 31/4192A61K 31/695A61K 31/445A61K 31/535A61K 31/404A61P 35/00A61K 31/397C07D 265/28A61K 51/025
48
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Claims

Abstract

The present invention relates to an aryl ethene derivative, for inhibiting an estrogen-related receptor gamma (ERRγ) activity, a prodrug of same, a solvate of same, a stereoisomer of same or pharmaceutically acceptable salts of same, and a pharmaceutical composition containing same as an active ingredient.

Claims

exact text as granted — not AI-modified
1 . A pharmaceutical composition for treating thyroid cancer, comprising: the arylethene derivative represented by the following Chemical Formula 1: 
       
         
           
           
               
               
           
         
         wherein 
         L is (C6-C20)arylene, (C3-C20)heteroarylene, or (C3-C20)fused heterocycle; 
         R 1  is (C3-C20)heterocycloalkyl, (C3-C20)heteroaryl, —O—(CH 2 ) m —R 11 , —(CH 2 ) m —R 12 , —NH—(CH 2 ) m —R 13 , —NHCO—(CH 2 ) n —R 14 , or —SiR 16 R 17 —(CH 2 ) m —R 15 ; 
         R 11  to R 15  are independently of one another (C3-C20)heterocycloalkyl; 
         R 16  and R 17  are independently of each other (C1-C20)alkyl; 
         m is an integer of 1 to 3; and 
         n is an integer of 0 or 1; 
         Ar is (C6-C20)aryl or (C3-C20)heteroaryl, in which the aryl or heteroaryl of Ar may be further substituted by one or more selected from the group consisting of hydroxy, halogen, (C1-C20)alkyl, halo(C1-C20)alkyl, (C1-C20)alkoxy, nitro, cyano, —NR 21 R 22 , (C1-C20)alkylcarbonyloxy, (C1-C20)alkylcarbonylamino, guanidino, —SO 2 —R 23 , and —OSO 2 —R 24 ; 
         R 21  and R 22  are independently of each other hydrogen, (C1-C20)alkylsulfonyl, or (C3-C20)cycloalkylsulfonyl; 
         R 23  and R 24  are independently of each other (C1-C20)alkyl, halo(C1-C20)alkyl, or (C3-C20)cycloalkyl; 
         R 2  is hydroxy, halogen, (C1-C20)alkylcarbonyloxy, or (C1-C20)alkylsulfonyloxy; 
         the heterocycloalkyl or heteroaryl of R 1  and the heterocycloalkyl of R 11  to R 15  may be further substituted by one or more selected from the group consisting of (C1-C20)alkyl, (C3-C20)cycloalkyl, (C2-C20)alkenyl, amidino, (C1-C20)alkoxycarbonyl, hydroxy, hydroxy(C1-C20)alkyl, and di(C1-C20)alkylamino(C1-C20)alkyl; and 
         the heterocycloalkyl and heteroaryl contains one or more heteroatoms selected from the group consisting of N, O and S, and the heterocycloalkyl is a saturated or unsaturated mono-, bi-, or spirocycle having a carbon atom or nitrogen atom in a ring as a binding site, 
         or a prodrug, solvate, stereoisomer, or pharmaceutically acceptable salt thereof, as an effective component, and a pharmaceutically acceptable carrier, and being used in combination of radioactive iodine. 
       
     
     
         2 . The pharmaceutical composition of  claim 1 , wherein the thyroid cancer is analpastic thyroid cancer. 
     
     
         3 . The pharmaceutical composition of  claim 1 , wherein the arylethene derivative is an arylethene derivative represented by the following Chemical Formulae 2 to 5: 
       
         
           
           
               
               
           
         
       
       wherein   denotes a single bond or a double bond; and R 1 , Ar and R 2  are as defined in  claim 1 . 
     
     
         4 . The pharmaceutical composition of  claim 1 , wherein
 R 1  is (C3-CO 1 )heterocycloalkyl, (C3-C10)heteroaryl, —O—(CH 2 ) m —R 11 , —(CH 2 ) m —R 12 , —NH—(CH 2 ) m —R 13 , —NHCO—(CH 2 ) n —R 14 , or —SiR 16 R 17 —(CH 2 ) m —R 15 ;   R 11  to R 15  are independently of one another (C3-C10)heterocycloalkyl;   R 16  and R 17  are independently of each other (C1-C10)alkyl;   m is an integer of 1 to 3;   n is an integer of 0 or 1;   Ar is (C6-C12)aryl or (C3-C12)heteroaryl, in which the aryl or heteroaryl of Ar may be further substituted by one or more selected from the group consisting of hydroxy, halogen, (C1-C10)alkyl, halo(C1-C10)alkyl, (C1-C10)alkoxy, nitro, cyano, amino, (C1-C10)alkylsulfonylamino, (C3-C10)cycloalkylsulfonylamino, di((C1-C10)alkylsulfonyl)amino, (C1-C10)alkylcarbonyloxy, (C1-C10)alkylcarbonylamino, guanidino, (C1-C10)alkylsulfonyl, (C1-C10)alkylsulfonyloxy, halo(C1-C10)alkylsulfonyloxy, and (C3-C10)cycloalkylsulfonyloxy;   R 2  is hydroxy, fluoro, (C1-C10)alkylcarbonyloxy, or (C1-C10)alkylsulfonyloxy; and   the heterocycloalkyl or heteroaryl of R 1  and the heterocycloalkyl of R 11  to R 15  may be further substituted by one or more selected from the group consisting of (C1-C10)alkyl, (C3-C10)cycloalkyl, (C2-C10)alkenyl, amidino, (C1-C10)alkoxycarbonyl, hydroxy(C1-C10)alkyl, and di(C1-C10)alkylamino(C1-C10)alkyl.   
     
     
         5 . The pharmaceutical composition of  claim 4 , wherein
 R 1  is (C3-C10)heterocycloalkyl or —O—(CH 2 ) m —R 11 ; R 11  is (C3-C10)heterocycloalkyl; m is an integer of 1 to 3; and the heterocycloalkyl of R 1  and R 11  may be further substituted by one or more selected from the group consisting of (C1-C10)alkyl, (C3-C10)cycloalkyl, (C2-C10)alkenyl, amidino, (C1-C10)alkoxycarbonyl, hydroxy(C1-C10)alkyl, and di(C1-C10)alkylamino(C1-C10)alkyl.   
     
     
         6 . The pharmaceutical composition of  claim 1 , wherein the heterocycloalkyl of R 1  and R 11  to R 15  is independently of each other selected from the following structures: 
       
         
           
           
               
               
           
         
       
       wherein R 31  and R 32  are independently of each other hydrogen, (C1-C10)alkyl, (C3-C10)cycloalkyl, (C2-C10)alkenyl, amidino, (C1-C10)alkoxycarbonyl, hydroxy(C1-C10)alkyl, or di(C1-C10)alkylamino(C1-C10)alkyl; and L is O or S. 
     
     
         7 . The pharmaceutical composition of  claim 3 , wherein the arylethene derivative is an arylethene derivative represented by the following Chemical Formula 6: 
       
         
           
           
               
               
           
         
         wherein 
         R 1  is (C3-C10)heterocycloalkyl or —O—(CH 2 ) m —R 1 ; 
         R 11  is (C3-C10)heterocycloalkyl; 
         m is an integer of 1 to 3; 
         the heterocycloalkyl of R 1  and R 11  may be further substituted by one or more selected from the group consisting of (C1-C10)alkyl, (C3-C10)cycloalkyl, (C2-C10)alkenyl, amidino, (C1-C10)alkoxycarbonyl, hydroxy(C1-C10)alkyl, and di(C1-C20)alkylamino(C1-C20)alkyl; 
         Ar is (C6-C12)aryl or (C3-C12)heteroaryl, in which the aryl or heteroaryl of Ar may be further substituted by one or more selected from the group consisting of hydroxy, halogen, (C1-C10)alkyl, halo(C1-C10)alkyl, (C1-C10)alkoxy, nitro, cyano, amino, (C1-C10)alkylsulfonylamino, (C3-C10)cycloalkylsulfonylamino, di((C1-C10)alkylsulfonyl)amino, (C1-C10)alkylcarbonyloxy, (C1-C10)alkylcarbonylamino, guanidino, (C1-C10)alkylsulfonyl, (C1-C10)alkylsulfonyloxy, halo(C1-C10)alkylsulfonyloxy, and (C3-C10)cycloalkylsulfonyloxy; and 
         R 2  is hydroxy, fluoro, (C1-C10)alkylcarbonyloxy, or (C1-C10)alkylsulfonyloxy. 
       
     
     
         8 . The pharmaceutical composition of  claim 7 , wherein R 2  is hydroxy; and R 1  is heterocycloalkyl selected from the following structures: 
       
         
           
           
               
               
           
         
       
       wherein R 31  and R 32  are independently of each other hydrogen, (C1-C10)alkyl, (C3-C10)cycloalkyl, (C2-C10)alkenyl, amidino, (C1-C10)alkoxycarbonyl, hydroxy(C1-C10)alkyl, or di(C1-C10)alkylamino(C1-C10)alkyl; and L is O or S. 
     
     
         9 . The pharmaceutical composition of  claim 7 , wherein R 2  is hydroxy; R 1  is —O—(CH 2 ) m —R 11 ; m is an integer of 1 or 2; and R 11  is heterocycloalkyl selected from the following structures: 
       
         
           
           
               
               
           
         
       
       wherein R 31  and R 32  are independently of each other halogen, (C1-C100)alkyl, (C1-C10)alkoxycarbonyl, or hydroxy(C1-C10)alkyl; and L is O or S. 
     
     
         10 . The pharmaceutical composition of  claim 3 , wherein the arylethene derivative is selected from the following structures: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
     
     
         11 . The pharmaceutical composition of  claim 7 , wherein the arylethene derivative is selected from the following structures: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
     
     
         12 . A kit for treating thyroid cancer, comprising: an arylethene derivative represented by the following Chemical Formula 1: 
       
         
           
           
               
               
           
         
         wherein 
         L is (C6-C20)arylene, (C3-C20)heteroarylene, or (C3-C20)fused heterocycle; 
         R 1  is (C3-C20)heterocycloalkyl, (C3-C20)heteroaryl, —O—(CH 2 ) m —R 11 , —(CH 2 ) m —R 12 , —NH—(CH 2 ) m —R 13 , —NHCO—(CH 2 ) n —R 14 , or —SiR 16 R 17 —(CH 2 ) m —R 15 ; 
         R 11  to R 15  are independently of one another (C3-C20)heterocycloalkyl; 
         R 16  and R 17  are independently of each other (C1-C20)alkyl; 
         m is an integer of 1 to 3; 
         n is an integer of 0 or 1; 
         Ar is (C6-C20)aryl or (C3-C20)heteroaryl, in which the aryl or heteroaryl of Ar may be further substituted by one or more selected from the group consisting of hydroxy, halogen, (C1-C20)alkyl, halo(C1-C20)alkyl, (C1-C20)alkoxy, nitro, cyano, —NR 21 R 22 , (C1-C20)alkylcarbonyloxy, (C1-C20)alkylcarbonylamino, guanidino, —SO 2 —R 23  and —OSO 2 —R 24 ; 
         R 21  and R 22  are independently of each other hydrogen, (C1-C20)alkylsulfonyl, or (C3-C20)cycloalkylsulfonyl; 
         R 23  and R 24  are independently of each other (C1-C20)alkyl, halo(C1-C20)alkyl, or (C3-C20)cycloalkyl; 
         R 2  is hydroxy, halogen, (C1-C20)alkylcarbonyloxy, or (C1-C20)alkylsulfonyloxy; 
         the heterocycloalkyl or heteroaryl of R 1  and the heterocycloalkyl of R 11  to R 15  may be further substituted by one or more selected from the group consisting of (C1-C20)alkyl, (C3-C20)cycloalkyl, (C2-C20)alkenyl, amidino, (C1-C20)alkoxycarbonyl, hydroxy, hydroxy(C1-C20)alkyl, and di(C1-C20)alkylamino(C1-C20)alkyl; and 
         the heterocycloalkyl and heteroaryl contains one or more heteroatoms selected from the group consisting of N, O and S, and the heterocycloalkyl is a saturated or unsaturated mono-, bi-, or spirocycle having a carbon atom or nitrogen atom in a ring as a binding site, 
         or a prodrug, solvate, stereoisomer, or pharmaceutically acceptable salt thereof, and radioactive iodine.

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