US2018230012A1PendingUtilityA1

Method of producing spherical boron nitride fine particles

Assignee: DENKA COMPANY LTDPriority: Feb 12, 2014Filed: Apr 17, 2018Published: Aug 16, 2018
Est. expiryFeb 12, 2034(~7.5 yrs left)· nominal 20-yr term from priority
C01P 2004/62C01P 2006/80C01B 21/0646C01P 2004/64C01P 2004/03C01P 2004/04C01P 2004/32
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Claims

Abstract

A method of producing a spherical boron nitride fine particle includes reacting ammonia with an alkoxide borate at an ammonia/alkoxide borate molar ratio of 1 to 10 in an inert gas stream at 750° C. or higher within 30 seconds, then applying heat treatment to a reaction product in an atmosphere of ammonia gas or a mixed gas of ammonia gas and an inert gas at 1,000 to 1,600° C. for at least 1 hour, and further firing the reaction product in an inert gas atmosphere at 1,800 to 2,200° C. for at least 0.5 hour.

Claims

exact text as granted — not AI-modified
What is claimed is: 
     
         1 . A method of producing a spherical boron nitride fine particle, characterized by reacting ammonia with an alkoxide borate at an ammonia/alkoxide borate molar ratio of 1 to 10 in an inert gas stream at 750° C. or higher within 30 seconds, then applying heat treatment to a reaction product in an atmosphere of ammonia gas or a mixed gas of ammonia gas and an inert gas at 1,000 to 1,600° C. for at least 1 hour, and further firing the reaction product in an inert gas atmosphere at 1,800 to 2,200° C. for at least 0.5 hour.

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