Method for producing magnesium alcoholate
Abstract
The purpose of the present invention is to provide a spherical or ellipsoidal magnesium alcoholate having a narrow particle size distribution even when the particle size is small. The present invention provides a method for producing a magnesium alcoholate by adding in a portionwise manner to a reaction system and reacting, metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound in the reaction system under alcohol reflux, which is a method for producing a magnesium alcoholate characterized in that a mixture of metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound is added to the reaction system at each portionwise addition.
Claims
exact text as granted — not AI-modified1 . A method for producing a magnesium alcoholate comprising:
adding in a portionwise manner to a reaction system and reacting, metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound in a reaction system under alcohol reflux, wherein a mixture of metallic magnesium, an alcohol, and at least one of a halogen or a halogen atom-containing compound is added to the reaction system at each portionwise addition.
2 . The method for producing a magnesium alcoholate according to claim 1 , wherein a frequency of portionwise addition of said mixture is less than 10 times.
3 . The method for producing a magnesium alcoholate according to claim 1 ,
wherein a mass ratio of metallic magnesium and alcohol and a mass ratio of metallic magnesium and halogen or halogen atom-containing compound in said mixture that is added in a portionwise manner is set to be substantially constant at each portionwise addition.
4 . The method for producing a magnesium alcoholate according to claim 1 ,
wherein an interval of portionwise addition of said mixture is set to be substantially constant.
5 . The method for producing a magnesium alcoholate according to claim 1 ,
wherein the halogen or the halogen-containing compound is reacted in an amount of 0.0001 gram atom or more, relative to one gram atom of the metallic magnesium.
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