US2016145117A1PendingUtilityA1

Nanocrystaline spherical ceramic oxides, process for the synthesis and use thereof

Assignee: CUF COMPANHIA UNIAO FABRIL SGPS S APriority: Sep 28, 2007Filed: Jan 7, 2016Published: May 26, 2016
Est. expirySep 28, 2027(~1.2 yrs left)· nominal 20-yr term from priority
C01P 2004/32C01F 7/02C01P 2004/61C01G 23/053C01G 23/047C01F 7/42C01P 2004/53C01P 2002/60C01G 23/04C01G 3/02C01F 5/04C01F 5/02C01B 33/18C01B 33/12C01B 13/328C01B 13/185C01B 13/18B01J 3/08C01P 2004/64C01P 2006/32C01G 45/02C01G 53/04C01P 2006/80C01G 25/02Y10T428/2982C01G 9/02
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Claims

Abstract

The present invention refers to nanocrystaline spherical ceramic oxides, to the process for the synthesis and use thereof. These oxides, obtained by detonation of a water-in-oil emulsion (W/O), besides having a spherical morphology and nanocrystallinity, show a set of complementary features, namely a particle dimension inferior to 40 μm, bimodal particle size distribution, high purity, deagglomeration and stable crystalline stages. This set of features makes these powders particularly suitable for several applications such as coating processes, near net shape processes and, when applied in ceramics industry, they provide dense and porous ceramic objects of exceptionally high mechanical resistance.

Claims

exact text as granted — not AI-modified
1 - 9 . (canceled) 
     
     
         10 . Powder nanocrystaline spherical ceramic oxides, comprising:
 a) bimodal particle size distribution;   b) 99.5% purity;   c) deagglomerated particles;   d) stable crystalline stages; and   e) particle dimension inferior to 40 μm;   wherein the powder nanocrystaline spherical ceramic oxides are obtained by a process comprising detonating a water-in-oil emulsion (W/O) comprising metals, at temperatures in the point C, J (Chapman, Jouguet) higher than the oxide melting point, through control of the emulsion composition.   
     
     
         11 . Use of the nanocrystaline spherical ceramic oxides according to  claim 10 , wherein the nanocrystaline spherical ceramic oxides are applied in near net shape processes, preferably injection moulding, slip casting and coating. 
     
     
         12 . Use of the nanocrystaline spherical ceramic oxides according to  claim 11 , wherein the use is aimed for application in ceramic objects or as reinforcement matrixes.

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