US2011190323A1PendingUtilityA1

Cortistatin analogues and syntheses thereof

Assignee: HARVARD COLLEGEPriority: Aug 28, 2008Filed: Aug 28, 2009Published: Aug 4, 2011
Est. expiryAug 28, 2028(~2.1 yrs left)· nominal 20-yr term from priority
A61P 35/00A61K 31/4725A61K 31/34C07D 493/08
64
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Claims

Abstract

The present invention relates to analogs of cortistatin A, J, K, and L, having the general formula: I and salts thereof, wherein R 1 , R 2 , R 3 , R 4 , n, and m are as defined herein; processes for preparing such compounds and intermediates thereto; pharmaceutical compositions comprising such compounds; methods for treating a proliferative disease; methods for treating a disease associated with aberrant angiogenesis; methods for inhibiting angiogenesis; and processes for preparing cortistatin A, J, K, and L, and analogs thereof.

Claims

exact text as granted — not AI-modified
1 . A compound of formula: 
       
         
           
           
               
               
           
         
         wherein:
 each of the dashed lines independently represents the presence or absence of a bond; 
 m is an integer between 0 and 6, inclusive; 
 n is an integer between 0 and 8, inclusive; 
 each occurrence of R 1  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR A ; —C(═O)R A ; —CO 2 R A ; —CN; —SCN; —SR A ; —SOR A ; —SO 2 R A ; —NO 2 ; —N 3 ; ═O; ═N(R A ); ═S; —N(R A ) 2 ; —NHC(═O)R A ; —NR A C(═O)N(R A ) 2 ; —OC(═O)OR A ; —OC(═O)R A ; —OC(═O)N(R A ) 2 ; —NR A C(═O)OR A ; or —C(R A ) 3 ; wherein each occurrence of R A  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; or heteroarylthio moiety; 
 R 2  is hydrogen or C 1 -C 6  aliphatic; 
 R 3  is hydrogen or C 1 -C 6  aliphatic; 
 each occurrence of R 4  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR D ; —C(═O)R D ; —CO 2 R D ; —CN; —SCN; —SR S ; —SOR A ; —SO 2 R D ; —NO 2 ; —N 3 ; ═O; ═N(R D ); ═S; —N(R D ) 2 ; —NHC(═O)R D ; —NR A C(═O)N(R D ) 2 ; —OC(═O)OR D ; —OC(═O)R D ; —OC(═O)N(R D ) 2 ; —NR D C(═O)OR D ; or —C(R D ) 3 ; wherein each occurrence of R D  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; heteroarylthio; a 
 
       
       
         
           
           
               
               
           
         
       
       moiety; or a 
       
         
           
           
               
               
           
         
       
       moiety wherein z is an integer between 2 and 10, inclusive; provided that the compound is not any of the following formulae: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         and pharmaceutically acceptable salts thereof. 
       
     
     
         2 . The compound of  claim 1 , wherein m is 1. 
     
     
         3 . The compound of  claim 1 , wherein R 1  is aryl. 
     
     
         4 . The compound of  claim 1 , wherein R 1  is heteroaryl. 
     
     
         5 . The compound of  claim 4 , wherein R 1  is isoquinolinyl, naphthyl or quinazolinyl. 
     
     
         6 . The compound of  claim 1 , wherein R 1  is alkyl. 
     
     
         7 . The compound of  claim 1 , wherein R 2  is methyl. 
     
     
         8 . The compound of  claim 1 , wherein R 3  is hydrogen. 
     
     
         9 . The compound of  claim 1 , wherein n is 1, 2, or 3. 
     
     
         10 - 11 . (canceled) 
     
     
         12 . The compound of  claim 1 , wherein R 4  is —OR D . 
     
     
         13 . The compound of  claim 1 , wherein R 4  is —N(R D ) 2 . 
     
     
         14 . The compound of  claim 13 , wherein each R D  is methyl. 
     
     
         15 . (canceled) 
     
     
         16 . The compound of  claim 1  of formula: 
       
         
           
           
               
               
           
         
       
     
     
         17 - 18 . (canceled) 
     
     
         19 . The compound of  claim 1  of formula: 
       
         
           
           
               
               
           
         
       
     
     
         20 . The compound of  claim 1  of formula: 
       
         
           
           
               
               
           
         
       
     
     
         21 . (canceled) 
     
     
         22 . The compound of  claim 1 , wherein said compound is of formula: 
       
         
           
           
               
               
           
         
       
     
     
         23 . (canceled) 
     
     
         24 . The compound of  claim 22  of formula: 
       
         
           
           
               
               
           
         
       
     
     
         25 - 26 . (canceled) 
     
     
         27 . The compound of  claim 1  of formula: 
       
         
           
           
               
               
           
         
       
     
     
         28 - 61 . (canceled) 
     
     
         62 . A method of treating a condition associated with aberrant angiogenesis, comprising the step of administering a therapeutically effective amount of a compound of formula: 
       
         
           
           
               
               
           
         
         wherein:
 each of the dashed lines independently represents the presence or absence of a bond; 
 m is an integer between 0 and 6, inclusive; 
 n is an integer between 0 and 8, inclusive; 
 each occurrence of R 1  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR A ; —C(═O)R A ; —CO 2 R A ; —CN; —SCN; —SR A ; —SOR A ; —SO 2 R A ; —NO 2 ; —N 3 ; ═O; ═N(R A ); ═S; —N(R A ) 2 ; —NHC(═O)R A ; —NR A C(═O)N(R A ) 2 ; —OC(═O)OR A ; —OC(═O)R A ; —OC(═O)N(R A ) 2 ; —NR A C(═O)OR A ; or —C(R A ) 3 ; wherein each occurrence of R A  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; or heteroarylthio moiety; 
 R 2  is hydrogen or C 1 -C 6  aliphatic; 
 R 3  is hydrogen or C 1 -C 6  aliphatic; 
 each occurrence of R 4  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR D ; —C(═O)R D ; —CO 2 R D ; —CN; —SCN; —SR D ; —SOR D ; —SO 2 R D ; —NO 2 ; —N 3 ; ═O; ═N(R D ); ═S; —N(R D ) 2 ; —NHC(═O)R D ; —NR A C(═O)N(R D ) 2 ; —OC(═O)OR D ; —OC(═O)R D ; —OC(═O)N(R D ) 2 ; —NR D C(═O)OR D ; or —C(R D ) 3 ; wherein each occurrence of R D  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; heteroarylthio; a 
 
       
       
         
           
           
               
               
           
         
       
       moiety; or a 
       
         
           
           
               
               
           
         
       
       moiety wherein z is an integer between 2 and 10, inclusive; provided that the compound is not any of the following formulae: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         to a subject. 
       
     
     
         63 . A method of treating a proliferative disease, comprising the step of administering a therapeutically effective amount of a compound of formula: 
       
         
           
           
               
               
           
         
         wherein:
 each of the dashed lines independently represents the presence or absence of a bond; 
 m is an integer between 0 and 6, inclusive; 
 n is an integer between 0 and 8, inclusive; 
 each occurrence of R 1  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR A ; —C(═O)R A ; —CO 2 R A ; —CN; —SCN; —SR A ; —SOR A ; —SO 2 R A ; —NO 2 ; —N 3 ; ═O; ═N(R A ); ═S; —N(R A ) 2 ; —NHC(═O)R A ; —NR A C(═O)N(R A ) 2 ; —OC(═O)OR A ; —OC(═O)R A ; —OC(═O)N(R A ) 2 ; —NR A C(═O)OR A ; or —C(R A ) 3 ; wherein each occurrence of R A  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; or heteroarylthio moiety; 
 R 2  is hydrogen or C 1 -C 6  aliphatic; 
 R 3  is hydrogen or C 1 -C 6  aliphatic; 
 each occurrence of R 4  is independently selected from the group consisting of hydrogen; halogen; cyclic or acyclic, substituted or unsubstituted, branched or unbranched aliphatic; cyclic or acyclic, substituted or unsubstituted, branched or unbranched heteroaliphatic; substituted or unsubstituted, branched or unbranched acyl; substituted or unsubstituted, branched or unbranched aryl; substituted or unsubstituted, branched or unbranched heteroaryl; —OR D ; —C(═O)R D ; —CO 2 R D ; —CN; —SCN; —SR S ; —SOR A ; —SO 2 R D ; —NO 2 ; —N 3 ; ═O; ═N(R D ); ═S; —N(R D ) 2 ; —NHC(═O)R D ; —NR A C(═O)N(R D ) 2 ; —OC(═O)OR D ; —OC(═O)R D ; —OC(═O)N(R D ) 2 ; —NR D C(═O)OR D ; or —C(R D ) 3 ; wherein each occurrence of R D  is independently a hydrogen, a protecting group, an aliphatic moiety, a heteroaliphatic moiety, an acyl moiety; an aryl moiety; a heteroaryl moiety; alkoxy; aryloxy; alkylthio; arylthio; amino, alkylamino, dialkylamino, heteroaryloxy; heteroarylthio; a 
 
       
       
         
           
           
               
               
           
         
       
       moiety; or a 
       
         
           
           
               
               
           
         
       
       moiety wherein z is an integer between 2 and 10, inclusive; provided that the compound is not any of the following formulae: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         to a subject. 
       
     
     
         64 - 107 . (canceled)

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