US2010089499A1PendingUtilityA1

Method of manufacturing metal coated with ceramic

Assignee: TOKAI CARBON KOREA CO LTDPriority: Jan 29, 2008Filed: Dec 14, 2009Published: Apr 15, 2010
Est. expiryJan 29, 2028(~1.5 yrs left)· nominal 20-yr term from priority
C23C 26/00C23C 18/1208C23C 18/1204C23C 28/042C23C 18/143C23C 18/1241C23C 18/145Y10T428/265C23C 28/00
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Claims

Abstract

A metal coated with ceramic and a method manufacturing the same. The metal contains chromium. A buffer layer is disposed on the metal, and a silicon carbide (SiC) coating layer is disposed on the buffer layer. The buffer layer has a thermal expansion coefficient between those of the metal and the SiC coating layer. The method includes annealing a metal containing chromium to form a chromium oxide layer on the metal, dissolving polycarbosilane (PCS) in a solvent to form a PCS coating solution, coating the chromium oxide layer with the PCS solution, and annealing the to form an SiC coating.

Claims

exact text as granted — not AI-modified
1 - 3 . (canceled) 
   
   
       4 . A method of manufacturing a metal coated with a ceramic comprising:
 a) annealing a metal containing chromium to form a chromium oxide layer on the metal;   b) dissolving polycarbosilane (PCS) in a solvent to form a PCS coating solution;   c) coating the chromium oxide layer with the PCS coating solution and drying the PCS coating solution to leave a PCS coating; and   d) annealing and transforming the PCS coating into a silicon carbide (SiC) coating.   
   
   
       5 . The method according to  claim 4 , wherein the metal containing chromium is one of Inconel and stainless steel. 
   
   
       6 . The method according to  claim 5 , wherein the metal containing chromium is Inconel and including oxidizing the Inconel for 2 to 3 hours at a temperature of 900° C. to 1100° C., so that the chromium oxide layer has a thickness of 0.1 μm to 9 μm. 
   
   
       7 . The method according to  claim 5 , wherein the metal containing chromium is stainless steel and including oxidizing the stainless steel for 2 to 3 hours at a temperature of 700° C. to 900° C., so that the chromium oxide layer has a thickness of 0.1 μm to 9 μm. 
   
   
       8 . The method according to  claim 4 , further comprising preprocessing the PCS coating between the coating and annealing steps to cross-link the PCS coating. 
   
   
       9 . The method according to  claim 8 , wherein the preprocessing includes at least one of irradiating the PCS coating with electron beams, irradiating the PCS coating with ultraviolet light, and oxidizing the PCS coating. 
   
   
       10 . (canceled)

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