US2009069371A1PendingUtilityA1

Isoquinoline compounds

Assignee: AERIE PHARMACEUTICALS INCPriority: Jul 11, 2005Filed: Nov 20, 2008Published: Mar 12, 2009
Est. expiryJul 11, 2025(expired)· nominal 20-yr term from priority
A61P 9/10A61P 9/12A61P 9/00A61P 37/08A61P 27/06A61P 27/02A61P 3/04A61P 35/00A61P 13/00A61P 19/00A61P 19/08A61P 1/18A61P 17/00A61P 1/16A61P 1/00A61P 13/12A61P 11/02A61P 15/08C07D 217/02A61P 13/10
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Claims

Abstract

Isoquinoline compounds with G are provided that influence, inhibit or reduce the action of a G-protein receptor kinase. Pharmaceutical compositions including therapeutically effective amounts of the isoquinoline compounds and pharmaceutically acceptable carriers are also provided. Various methods using the compounds and/or compositions to affect disease states or conditions such as cancer, osteoporosis and glaucoma are also provided.

Claims

exact text as granted — not AI-modified
1 . A compound according to Formula (I): 
     
       
         
         
             
             
         
       
     
     wherein A is a substituted or unsubstituted isoquinoline radical wherein the isoquinoline radical may be mono- or disubstituted with halogen, cyano, nitro or C 1 -C 4  alkyl;
 R 1 , R 2 , R 3 , R 4 , and R 5  are, independently, hydrogen; halogen; C 1 -C 8  alkyl; alkoxy; phenoxy, —OR 7 ; amino; nitro; cyano; aryl; C 1 -C 4  alkylaryl; heteroaryl; C 1 -C 4  alkyl heteroaryl; carbonylamino; thioalkyl; sulfonyl; sulfonylamino; acyl; or carboxyl; 
 R 7  is C 1 -C 4  alkyl, aryl, heteroaryl, C 1 -C 4  alkyl aryl or C 1 -C 4  alkyl heteroaryl; 
 X is O, S, S(O), S(O)(O), 
 
     
       
         
         
             
             
         
       
     
     R 6  is CH 2  or CH(C 1 -C 4  alkyl). 
   
   
       2 . A compound according to  claim 1  wherein X is 
     
       
         
         
             
             
         
       
     
   
   
       3 . A compound according to  claim 2  wherein R 1 , R 2 , R 3 , R 4 , and R 5  are not phenoxy. 
   
   
       4 . A compound according to  claim 3  wherein X is 
     
       
         
         
             
             
         
       
     
   
   
       5 . A compound according to  claim 4  wherein A is an unsubstituted isoquinoline radical and R 1 , R 3 , and R 5  are hydrogen. 
   
   
       6 . A compound according to  claim 4  wherein R 1 , R 2 , R 3 , and R 5  are hydrogen and R 4  is —O—R 7 . 
   
   
       7 . A compound according to  claim 4  wherein R 4  is carbonylamino, sulfylamino, acyl or carboxyl. 
   
   
       8 . A compound according to  claim 4  wherein R 1 , R 2 , and R 5  are H and one of R 3  and R 4  is carbonylamino, sulfylamino, acyl or carboxyl. 
   
   
       9 . A compound according to Formula II: 
     
       
         
         
             
             
         
       
     
     wherein R 1′ , R 2′ , R 3′ , R 4′ , and R 5′  are, independently, hydrogen; halogen; unsubstituted C 1 -C 4  alkyl; amino; nitro; cyano; carbonylamino; alkoxy; —O—R 7′ ; sulfonylamino; carboxyl; acyl; or thioalkyl;
 R 7′  is C 1 -C 4  alkyl, aryl, heteroaryl, C 1 -C 4  alkyl aryl or C 1 -C 4  alkyl heteroaryl; 
 X′ is O, S, S(O), S(O)(O), 
 
     
       
         
         
             
             
         
       
     
     R 6′  is CH 2  or CH(C 1 -C 4  alkyl). 
   
   
       10 . A compound according to  claim 9  wherein X′ is 
     
       
         
         
             
             
         
       
     
   
   
       11 . A compound according to  claim 9  wherein X′ is 
     
       
         
         
             
             
         
       
     
   
   
       12 . A compound according to  claim 9  wherein R 1′ , R 2′ , R 3′ , and R 5′  are hydrogen and R 4′ , is —O—R 7′ . 
   
   
       13 . A compound according to  claim 9  wherein R 4′  is carbonylamino, sulfylamino, acyl or carboxyl. 
   
   
       14 . A compound according to  claim 13  wherein R 4′  is carbonylamino, and the carbonylamino is C(O)NHphenyl, C(O)NH-m-pyridyl, C(O)NH-o-pyridyl, C(O)NH-p-pyridyl, C(O)NH 2 , or C(O)NHCH 3 . 
   
   
       15 . A compound according to  claim 9  wherein R 1′ , R 2′ , and R 5′  are H and one of R 3′  and R 4′  is carbonylamino, sulfylamino, acyl or carboxyl. 
   
   
       16 . A compound according  claim 11  wherein R 2′  or R 4′  is —O—R 7′ . 
   
   
       17 . A compound according to  claim 16  wherein R 7′  is methyl, ethyl, phenyl, benzyl, propyl or isopropyl. 
   
   
       18 . A method for influencing the action of a G-protein-coupled receptor kinase in a cell comprising administering to or contacting with the cell at least one compound according to Formula (II), or reducing GPCR desensitization in a cell comprising administering to or contacting with the cell a therapeutically effective amount of a compound according to Formula (II), or inhibiting the action of a G-protein-coupled receptor kinase comprising applying to a medium or contacting with a cell an effective inhibitory amount of a compound according to Formula (II): 
     
       
         
         
             
             
         
       
     
     wherein R 1′ , R 2′ , R 3′ , R 4′ , and R 5′  are, independently, hydrogen; halogen; unsubstituted C 1 -C 4  alkyl; amino; nitro; cyano; carbonylamino; alkoxy; —O—R 7′ ; sulfonylamino; carboxyl; acyl; or thioalkyl;
 R 7′  is C 1 -C 4  alkyl, aryl, heteroaryl, C 1 -C 4  alkyl aryl or C 1 -C 4  alkyl heteroaryl; 
 X′ is O, S, S(O), S(O)(O), 
 
     
       
         
         
             
             
         
       
     
     R 6′  is CH 2  or CH(C 1 -C 4  alkyl). 
   
   
       19 . The method according to  claim 18  wherein X′ is 
     
       
         
         
             
             
         
       
     
   
   
       20 . The method according to  claim 19  wherein R 1′ , R 3′ , and R 5′  are hydrogen. 
   
   
       21 . The method according  claim 20  wherein R 2′  or R 4′  is —O—R 7′ . 
   
   
       22 . The method according to  claim 21  wherein R 7′  is methyl, ethyl, phenyl, benzyl, propyl or isopropyl. 
   
   
       23 . The method according to  claim 20  wherein R 2′  or R 4′  is carbonylamino. 
   
   
       24 . The method according to  claim 23  wherein the carbonylamino moiety is selected from C(O)NHphenyl, C(O)NH-m-pyridyl, C(O)NH-o-pyridyl, C(O)NH-p-pyridyl, C(O)NH 2 , or C(O)NHCH 3 . 
   
   
       25 . The method according to  claim 18  wherein the G-protein-coupled receptor kinase is GRK-2, GRK-3, GRK-5 or GRK-6. 
   
   
       26 . The method according to  claim 18  wherein the G-protein-coupled receptor kinase is GRK-2. 
   
   
       27 . A compound according to Formula III: 
     
       
         
         
             
             
         
       
     
     wherein R 8  and R 9  are independently hydrogen; halogen; unsubstituted C 1 -C 4  alkyl; substituted C 1 -C 4  alkyl; amino; nitro; cyano; carbonylamino; alkoxy; phenoxy, benzyloxy, —O—R 10 ; sulfonylamino; carboxyl; acyl; or thioalkyl; and
 R 10  is unsubstituted C 1 -C 4  alkyl; substituted C 1 -C 4  alkyl; substituted aryl, heteroaryl, substituted heteroaryl, C 1 -C 4  alkaryl or C 1 -C 4  alkheteroaryl. 
 
   
   
       28 . A compound according to  claim 27  wherein R 8  is carbonylamino, a carboxyl, a sulfonyl amino, a cyano, or an acyl moiety, and R 9  is selected from H, methyl, cyano, or halogen. 
   
   
       29 . A compound according to  claim 28  wherein R 8  is the carbonylamino, and the carbonylamino is C(O)NHphenyl, C(O)NH-m-pyridyl, C(O)NH-o-pyridyl, C(O)NH-p-pyridyl, C(O)NH 2 , and C(O)NHCH 3 . 
   
   
       30 . A compound according to  claim 28  wherein R 8  is the carboxyl and the carboxyl is C(O)O phenyl, C(O)O-m-pyridyl, C(O)O-o-pyridyl, C(O)O-p-pyridyl, C(O)NH 2 , or C(O)OCH 3 . 
   
   
       31 . A compound according to  claim 28  wherein R 8  is the sulfonyl amino, and the sulfonyl amino is S(O) 2 NHphenyl, S(O) 2 NH-m-pyridyl, S(O) 2 NH-o-pyridyl, S(O) 2 NH-p-pyridyl, S(O) 2 NH 2 , or S(O) 2 NHCH 3 . 
   
   
       32 . A compound according to  claim 27  wherein R 9  is a carbonylamino, a carboxyl, a sulfonyl amino, a cyano, or an acyl moiety, and R 8  is H, methyl, cyano, or halogen. 
   
   
       33 . A compound according to  claim 27  wherein R 8  is alkoxy, phenoxy, benzyloxy, or —O—R 10  and R 9  is H, methyl, cyano, or halogen. 
   
   
       34 . A compound according to  claim 27  wherein R 8  and R 9  are not phenoxy. 
   
   
       35 . A pharmaceutical composition comprising:
 a) an isoquinoline derivative having the structure   
     
       
         
         
             
             
         
       
     
     wherein R 8  and R 9  are independently hydrogen; halogen; unsubstituted C 1 -C 4  alkyl; substituted C 1 -C 4  alkyl; amino; nitro; cyano; carbonylamino; alkoxy; phenoxy, benzyloxy, —O—R 10 ; sulfonylamino; carboxyl; acyl; or thioalkyl; and 
     R 10  is unsubstituted C 1 -C 4  alkyl; substituted C 1 -C 4  alkyl; substituted aryl, heteroaryl, substituted heteroaryl, C 1 -C 4  alkaryl or C 1 -C 4  alkheteroaryl; and
 b) a carrier. 
 
   
   
       36 . The composition of  claim 35 , wherein the carrier is selected from the group consisting of systemic and topical carriers. 
   
   
       37 . The composition of  claim 35 , wherein the composition comprises about 0.01% to 10% of the isoquinoline derivative and 90 to 99.99% of the systemic carrier. 
   
   
       38 . A method of treating a condition comprising administering to a subject in need of treatment a safe and effective amount of an isoquinoline derivative, wherein the condition is selected from the group consisting of eye disease, bone disorder, heart disease, hepatic disease, renal disease, pancreatitis, cancer, myocardial infarct, gastric disturbance, hypertension, fertility control, nasal congestion, neurogenic bladder disorder, gastrointestinal disorder, and dermatological disorder. 
   
   
       39 . The method of  claim 38 , wherein the condition comprises eye disease. 
   
   
       40 . The method of  claim 39 , wherein the condition comprises glaucoma. 
   
   
       41 . The method of  claim 40 , wherein the isoquinoline derivative is of the Formula (I): 
     
       
         
         
             
             
         
       
     
     wherein A is a substituted or unsubstituted isoquinoline radical wherein the isoquinoline radical may be mono- or disubstituted with halogen, cyano, nitro or C 1 -C 4  alkyl;
 R 1 , R 2 , R 3 , R 4 , and R 5  are, independently, hydrogen; halogen; C 1 -C 8  alkyl; alkoxy; phenoxy, —O—R 7 ; amino; nitro; cyano; aryl; C 1 -C 4  alkylaryl; heteroaryl; C 1 -C 4  alkyl heteroaryl; carbonylamino; thioalkyl; sulfonyl; sulfonylamino; acyl; or carboxyl; 
 R 7  is C 1 -C 4  alkyl, aryl, heteroaryl, C 1 -C 4  alkyl aryl or C 1 -C 4  alkyl heteroaryl; 
 X is O, S, S(O), S(O)(O), 
 
     
       
         
         
             
             
         
       
     
     R 6  is CH 2  or CH(C 1 -C 4  alkyl). 
   
   
       42 . The method of  claim 41  wherein X is 
     
       
         
         
             
             
         
       
     
   
   
       43 . The method of  claim 42  wherein R 1 , R 2 , R 3 , R 4 , and R 5  are not phenoxy. 
   
   
       44 . The method of  claim 40  wherein the isoquinoline derivative is according to Formula II: 
     
       
         
         
             
             
         
       
     
     wherein R 1′ , R 2′ , R 3′ , R 4′ , and R 5′  are, independently, hydrogen; halogen; unsubstituted C 1 -C 4  alkyl; amino; nitro; cyano; carbonylamino; alkoxy; —O—R 7′ ; sulfonylamino; carboxyl; acyl; or thioalkyl;
 R 7′  is C 1 -C 4  alkyl, aryl, heteroaryl, C 1 -C 4  alkyl aryl or C 1 -C 4  alkyl heteroaryl; 
 X′ is O, S, S(O), S(O)(O), 
 
     
       
         
         
             
             
         
       
     
     R 6′  is CH 2  or CH(C 1 -C 4  alkyl). 
   
   
       45 . A method according to  claim 44  wherein X′ is 
     
       
         
         
             
             
         
       
     
   
   
       46 . A method according to  claim 44  wherein X′ is 
     
       
         
         
             
             
         
       
     
   
   
       47 . A compound selected from the following:

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