US2008293321A1PendingUtilityA1
Fabrication method of field emitter electrode
Est. expirySep 14, 2024(expired)· nominal 20-yr term from priority
H01J 9/025H01J 1/304B82Y 10/00B82Y 30/00H01J 2201/30469B82Y 40/00
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Claims
Abstract
A process for fabricating a field emitter electrode includes: impregnating a cathode and anode in an electrolyte containing carbon nanotubes dispersed therein and applying a predetermined voltage to the cathode and anode so as to deposit carbon nanotubes on a substrate provided on the anode; recovering the substrate and applying a conductive polymer onto the surface of the substrate having carbon nanotubes deposited thereon; and heat treating the conductive polymer having carbon nanotubes deposited thereon, so as to completely cure it.
Claims
exact text as granted — not AI-modified1 . A process for fabricating a field emitter electrode, comprising the steps of:
impregnating a cathode and anode in an electrolyte containing carbon nanotubes dispersed therein and applying a predetermined voltage to the cathode and anode so as to deposit carbon nanotubes on a substrate provided on either of two electrodes; recovering the substrate and applying a conductive polymer onto the surface of the substrate having carbon nanotubes deposited thereon; and heat treating them to cure the conductive polymer.
2 . The process as set forth in claim 1 , wherein the carbon nanotubes have a length of 1 to 2 μm.
3 . The process as set forth in claim 1 , wherein the applied conductive polymer layer has a thickness of about 0.2 to 1 μm.
4 . The process as set forth in claim 1 , wherein the conductive polymer is selected from the group consisting of polypyrrol, polyaniline, poly(3,4-ethylenedioxythiophene), polyacetylene, poly(p-phenylene), polythiophene, poly(p-phenylenevinylene) and poly(thienylene vinylene).
5 . The process as set forth in claim 1 , wherein the step of applying the conductive polymer is performed by a process selected from the group consisting of spin coating, spray coating, screen printing and ink jet printing.
6 . The process as set forth in claim 1 , wherein a dispersing agent is additionally added to the electrolyte in which carbon nanotubes were dispersed.
7 . The process as set forth in claim 1 , wherein the dispersing agent is at least one cationic dispersing agent selected from benzene konium chloride, polyethyleneimine and magnesium chloride (MgCl 2 ), or an anionic dispersing agent such as sodium dodecyl sulfate.
8 . The process as set forth in claim 7 , wherein the dispersing agent is added in an amount of about 100 wt % to about 500 wt % relative to the amount of carbon nanotubes.
9 . The process as set forth in claim 1 , further comprising:
more homogeneously dispersing the electrolyte in which carbon nanotubes were dispersed, using ultrasonic waves, prior to the step of depositing the carbon nanotubes.
10 . The process as set forth in claim 1 , further comprising:
etching the surface of the conductive polymer layer so as to sufficiently expose the carbon nanotubes.
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