Micron-size polymer particles, production and uses thereof
Abstract
A plurality of micron-size solid particles is described herein that includes at least one polyamide compound, wherein the particles comprise a diameter in the range of about 1 micron to about 1000 microns, and wherein at least some of the plurality of particles are substantially transparent. In addition, a plurality of micron-size solid particles is described herein that includes at least one polyamide compound, wherein the particles comprise a diameter of less than about 4 microns. Methods of forming a plurality of micron-size solid particles are also described that include a) introducing at least one amide-based compound having a melting point, at least one suspending agent and at least one surfactant into a reaction vessel to form a reaction mixture; b) applying a thermal energy to the reaction mixture, wherein the thermal energy comprises a temperature that is at or above the melting point of the at least one amide-based compound; c) polymerizing the at least one amide-based compound in the reaction mixture; d) cooling the reaction mixture; and e) rinsing the reaction mixture to retrieve the polymer particles.
Claims
exact text as granted — not AI-modified1 - 11 . (canceled)
12 . A method of forming a plurality of micron-size particles, comprising:
introducing at least one amide-based compound having a melting point, at least one suspending agent and at least one surfactant into a reaction vessel to form a reaction mixture; applying a thermal energy to the reaction mixture, wherein the thermal energy comprises a temperature that is at or above the melting point of the at least one amide-based compound; polymerizing the at least one amide-based compound in the reaction mixture; cooling the reaction mixture; and rinsing the reaction mixture to retrieve the polymer particles.
13 . The method of claim 12 , wherein the reaction mixture is made substantially free of moisture before the thermal energy is applied.
14 . The method of claim 12 , wherein polymerizing the at least one amide comprises introducing at least one alkylating agent.
15 . The method of claim 14 , wherein polymerizing the at least one amide further comprises introducing at least one activator.
16 . The method of claim 14 , wherein the at least one alkylating agent comprises sodium hydride.
17 . The method of claim 15 , wherein the at least one activator comprises a polyisocyanate compound.
18 . The method of claim 12 , wherein rinsing the reaction mixture comprises water.
19 . The method of claim 12 , wherein introducing further comprises introducing at least one nucleating agent.
20 . The method of claim 19 , wherein the nucleating agent comprises at least one inert particle.
21 . The method of claim 20 , wherein the inert particle comprises an alumina-silicate compound.
22 . The method of claim 20 , wherein in the inert particle comprises at least one color pigment.
23 . A polymer particle formed using the method of claim 12 .
24 . A polymer particle formed using the method of claim 14 .
25 . A polymer particle formed using the method of claim 15 .
26 . A polymer particle formed using the method of claim 19 .
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