US2005107404A1PendingUtilityA1

Mitotic kinesin inhibitors

Priority: Dec 6, 2001Filed: Dec 2, 2002Published: May 19, 2005
Est. expiryDec 6, 2021(expired)· nominal 20-yr term from priority
A61P 35/00C07D 239/70C07D 401/12C07D 403/06C07D 401/06C07D 401/14A61P 43/00
49
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Claims

Abstract

The present invention relates to cycloalkylpyrimidinone compounds that are useful for treating cellular proliferative diseases, for treating disorders associated with KSP kinesin activity, and for inhibiting KSP kinesin. The invention also related to compositions which comprise these compounds, and methods of using them to treat cancer in mammals.

Claims

exact text as granted — not AI-modified
1 . A compound of Formula I:  
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or stereoisomer thereof, wherein: 
 a is 0 or 1;  
 b is 0 or 1;  
 m is 0, 1, or 2;  
 n is 1 to 3;  
 r is 0 to 3;  
 u is 2, 3, 4 or 5;  
 R 1  is selected from: 
 1) H,  
 2) C 1 -C 10  alkyl,  
 3) aryl,  
 4) C 2 -C 10  alkenyl,  
 5) C 2 -C 10  alkynyl,  
 6) C 1 -C 6  perfluoroalkyl,  
 7) C 1 -C 6  aralkyl,  
 8) C 3 -C 8  cycloalkyl, and  
 9) heterocyclyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, aralkyl and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 R 2  and R 2′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) (C═O) a O b C 2 -C 10  alkenyl,  
 5) (C═O) a O b C 2 -C 10  alkynyl,  
 6) CO 2 H,  
 7) C 1 -C 6  perfluoroalkyl,  
 8) (C═O) a O b C 3 -C 8  cycloalkyl,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ; or  
 
 R 2  and R 2′  are combined to form —(CH 2 ) u — wherein one of the carbon atoms is optionally replaced by a moiety selected from O, S(O) m , —NC(O)—, and —N(R b )—, and wherein the ring formed when R 2  and R 2′  are combined is optionally substitued with one, two or three substituents selected from R 5 ;  
 R 3  and R 3′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) (C═O) a O b C 2 -C 10  alkenyl,  
 5) (C═O) a O b C 2 -C 10  alkynyl,  
 6) CO 2 H,  
 7) C 1 -C 6  perfluoroalkyl,  
 8) (C═O) a O b C 3 -C 8  cycloalkyl,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 or R 3  and R 3′  along with the nitrogen to which they are attached are combined to form ring  
                     
 which is a 5-12 membered nitrogen-containing heterocycle, which is optionally substituted with from one to six R 5  groups and which optionally incoporates from one to two additional heteroatoms, selected from N, O and S in the heterocycle ring;  
 R 4  is independently selected from: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) (C═O) a O b C 2 -C 10  alkenyl,  
 4) (C═O) a O b C 2 -C 10  alkynyl,  
 5) CO 2 H,  
 6) halo,  
 7) OH,  
 8) O b C 1 -C 6  perfluoroalkyl,  
 9) (C═O) a NR 7 R 8 ,  
 10) CN,  
 11) (C═O) a O b C 3 -C 8  cycloalkyl,  
 12) (C═O) a O b heterocyclyl,  
 13) SO 2 NR 7 R 8 , and  
 14) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 R 5  is: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) C 2 -C 10  alkenyl,  
 4) C 2 -C 10  alkynyl,  
 5) (C═O) a O b  heterocyclyl,  
 6) CO 2 H,  
 7) halo,  
 8) CN,  
 9) OH,  
 10) O b C 1 -C 6  perfluoroalkyl,  
 11) O a (C═O) b NR 7 R 8 ,  
 12) oxo,  
 13) CHO,  
 14) (N═O)R 7 R 8 , or  
 15) (C═O) a O b C 3 -C 8  cycloalkyl,  
 said alkyl, aryl, alkenyl, alkynyl, heterocyclyl, and cycloalkyl optionally substituted with one or more substituents selected from R 6 ;  
 
 R 6  is selected from: 
 1) (C═O) r O s (C 1 -C 10 )alkyl, wherein r and s are independently 0 or 1,  
 2) O r (C 1 -C 3 )perfluoroalkyl, wherein r is 0 or 1,  
 3) (C 0 -C 6 )alkylene-S(O) m R a , wherein m is 0, 1, or 2,  
 4) oxo,  
 5) OH,  
 6) halo,  
 7) CN,  
 8) (C═O) r O s (C 2 -C 10 )alkenyl,  
 9) (C═O) r O s (C 2 -C 10 )alkynyl,  
 10) (C═O) r O s (C 3 -C 6 )cycloalkyl,  
 11) (C═O) r O s (C 0 -C 6 )alkylene-aryl,  
 12) (C═O) r O s (C 0 -C 6 )alkylene-heterocyclyl,  
 13) (C═O) r O s (C 0 -C 6 )alkylene-N(R b )  
 14) C(O)R a ,  
 15) (C 0 -C 6 )alkylene-CO 2 R a ,  
 16) C(O)H,  
 17) (C 0 -C 6 )alkylene-CO 2 H, and  
 18) C(O)N(R b ) 2 ,  
 said alkyl, alkenyl, alkynyl, cycloalkyl, aryl, and heterocyclyl is optionally substituted with up to three substituents selected from R b , OH, (C 1 -C 6 )alkoxy, halogen, CO 2 H, CN, O(C═O)C 1 -C 6  alkyl, oxo, and N(R b ) 2 ;  
 
 R 7  and R 8  are independently selected from: 
 1) H,  
 2) (C═O)O b C 1 -C 10  alkyl,  
 3) (C═O)O b C 3 -C 8  cycloalkyl,  
 4) (C═O)O b aryl,  
 5) (C═O)O b heterocyclyl,  
 6) C 1 -C 10  alkyl,  
 7) aryl,  
 8) C 2 -C 10  alkenyl,  
 9) C 2 -C 10  alkynyl,  
 10) heterocyclyl,  
 11) C 3 -C 8  cycloalkyl,  
 12) SO 2 R a , and  
 13) (C═O)NR b   2 ,  
 said alkyl, cycloalkyl, aryl, heterocylyl, alkenyl, and alkynyl is optionally substituted with one or more substituents selected from R 6 , or  
 
 R 7  and R 8  can be taken together with the nitrogen to which they are attached to form a monocyclic or bicyclic heterocycle with 5-7 members in each ring and optionally containing, in addition to the nitrogen, one or two additional heteroatoms selected from N, O and S, said monocylcic or bicyclic heterocycle optionally substituted with one or more substituents selected from R 6 ;  
 R a  is (C 1 -C 6 )alkyl, (C 3 -C 6 )cycloalkyl, aryl, or heterocyclyl; and  
 R b  is H, (C 1 -C 6 )alkyl, aryl, heterocyclyl, (C 3 -C 6 )cycloalkyl, (C═O)OC 1 -C 6  alkyl, (C═O)C 1 -C 6  alkyl or S(O) 2 R a .  
 
     
     
         2 . A compound of Formula II:  
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or stereoisomer thereof, wherein: 
 a is 0 or 1;  
 b is 0 or 1;  
 m is 0, 1, or 2;  
 n is 1 to 3;  
 r is 0 to 3;  
 u is 2, 3, 4 or 5;  
 R 1  is selected from: 
 1) H,  
 2) C 1 -C 10  alkyl,  
 3) aryl,  
 4) C 2 -C 10  alkenyl,  
 5) C 2 -C 10  alkynyl,  
 6) C 1 -C 6  perfluoroalkyl,  
 7) C 1 -C 6  aralkyl,  
 8) C 3 -C 8  cycloalkyl, and  
 9) heterocyclyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, aralkyl and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 R 2  and R 2′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) (C═O) a O b C 2 -C 10  alkenyl,  
 5) (C═O) a O b C 2 -C 10  alkynyl,  
 6) CO 2 H,  
 7) C 1 -C 6  perfluoroalkyl,  
 8) (C═O) a O b C 3 -C 8  cycloalkyl,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ; or  
 
 R 2  and R 2′  are combined to form —(CH 2 ) u — wherein one of the carbon atoms is optionally replaced by a moiety selected from O, S(O) m , —NC(O)—, and —N(R b )—, and wherein the ring formed when R 2  and R 2′  are combined is optionally substtitued with one, two or three substituents selected from R 5 ;  
 R 3  and R 3′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) (C═O) a O b C 2 -C 10  alkenyl,  
 5) (C═O) a O b C 2 -C 10  alkynyl,  
 6) CO 2 H,  
 7) C 1 -C 6  perfluoroalkyl,  
 8) (C═O) a O b C 3 -C 8  cycloalkyl,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 or R 3  and R 3′  along with the nitrogen to which they are attached are combined to form ring  
                     
 which is a 5-12 membered nitrogen-containing heterocycle, which is optionally substituted with from one to six R 5  groups and which optionally incoporates from one to two additional heteroatoms, selected from N, O and S in the heterocycle ring;  
 R 4  is independently selected from: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) (C═O) a O b C 2 -C 10  alkenyl,  
 4) (C═O) a O b C 2 -C 10  alkynyl,  
 5) CO 2 H,  
 6) halo,  
 7) OH,  
 8) O b C 1 -C 6  perfluoroalkyl,  
 9) (C═O) a NR 7 R 8 ,  
 10) CN,  
 11) (C═O) a O b C 3 -C 8  cycloalkyl,  
 12) (C═O) a O b heterocyclyl,  
 13) SO 2 NR 7 R 8 , and  
 14) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one or more substituents selected from R 5 ;  
 
 R 5  is: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) C 2 -C 10  alkenyl,  
 4) C 2 -C 10  alkynyl,  
 5) (C═O) a O b  heterocyclyl,  
 6) CO 2 H,  
 7) halo,  
 8) CN,  
 9) OH,  
 10) O b C 1 -C 6  perfluoroalkyl,  
 11) O a (C═O) b NR 7 R 8 ,  
 12) oxo,  
 13) CHO,  
 14) (N═O)R 7 R 8 , or  
 15) (C═O) a O b C 3 -C 8  cycloalkyl,  
 said alkyl, aryl, alkenyl, alkynyl, heterocyclyl, and cycloalkyl optionally substituted with one or more substituents selected from R 6 ;  
 
 R 6  is selected from: 
 1) (C═O) r O s (C 1 -C 10 )alkyl, wherein r and s are independently 0 or 1,  
 2) O r (C 1 -C 3 )perfluoroalkyl, wherein r is 0 or 1,  
 3) (C 0 -C 6 )alkylene-S(O) m R a , wherein m is 0, 1, or 2,  
 4) oxo,  
 5) OH,  
 6) halo,  
 7) CN,  
 8) (C═O) r O s (C 2 -C 10 )alkenyl,  
 9) (C═O) r O s (C 2 -C 10 )alkynyl,  
 10) (C═O) r O s (C 3 -C 6 )cycloalkyl,  
 11) (C═O) r O s (C 0 -C 6 )alkylene-aryl,  
 12) (C═O) r O s (C 0 -C 6 )alkylene-heterocyclyl,  
 13) (C═O) r O s (C 0 -C 6 )alkylene-N(R b ) 2 ,  
 14) C(O)R a ,  
 15) (C 0 -C 6 )alkylene-CO 2 R a ,  
 16) C(O)H,  
 17) (C 0 -C 6 )alkylene-CO 2 H, and  
 18) C(O)N(R b ) 2 ,  
 said alkyl, alkenyl, alkynyl, cycloalkyl, aryl, and heterocyclyl is optionally substituted with up to three substituents selected from R b , OH, (C 1 -C 6 )alkoxy, halogen, CO 2 H, CN, O(C═O)C 1 -C 6  alkyl, oxo, and N(R b ) 2 ;  
 
 R 7  and R 8  are independently selected from: 
 1) H,  
 2) (C═O)O b C 1 -C 10  alkyl,  
 3) (C═O)O b C 3 -C 8  cycloalkyl,  
 4) (C═O)O b aryl,  
 5) (C═O)O b heterocyclyl,  
 6) C 1 -C 10  alkyl,  
 7) aryl,  
 8) C 2 -C 10  alkenyl,  
 9) C 2 -C 10  alkynyl,  
 10) heterocyclyl,  
 11) C 3 -C 8  cycloalkyl,  
 12) SO 2 R a , and  
 
 13) (C═O)NR b   2 ,  
 said alkyl, cycloalkyl, aryl, heterocylyl, alkenyl, and alkynyl is optionally substituted with one or more substituents selected from R 6 , or  
 R 7  and R 8  can be taken together with the nitrogen to which they are attached to form a monocyclic or bicyclic heterocycle with 5-7 members in each ring and optionally containing, in addition to the nitrogen, one or two additional heteroatoms selected from N, O and S, said monocylcic or bicyclic heterocycle optionally substituted with one or more substituents selected from R 6 ;  
 R a  is (C 1 -C 6 )alkyl, (C 3 -C 6 )cycloalkyl, aryl, or heterocyclyl; and  
 R b  is H, (C 1 -C 6 )alkyl, aryl, heterocyclyl, (C 3 -C 6 )cycloalkyl, (C═O)OC 1 -C 6  alkyl, (C═O)C 1 -C 6  alkyl or S(O) 2 R a .  
 
     
     
         3 . The compound according to  claim 2  or a pharmaceutically acceptable salt or stereoisomer thereof,  
       wherein: 
 a is 0 or 1;  
 b is 0 or 1;  
 m is 0, 1, or 2;  
 r is 0 to 2;  
 R 1  is selected from: 
 1) H,  
 2) C 1 -C 10  alkyl,  
 3) aryl,  
 4) C 1 -C 6  aralkyl,  
 5) C 3 -C 8  cycloalkyl, and  
 6) heterocyclyl,  
 said alkyl, aryl, cycloalkyl, aralkyl and heterocyclyl is optionally substituted with one, two or three substituents selected from R 5 ;  
 
 R 2  and R 2′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) CO 2 H,  
 5) C 1 -C 6  perfluoroalkyl,  
 6) (C═O) a O b C 3 -C 8  cycloalkyl, and  
 7) (C═O) a O b heterocyclyl,  
 said alkyl, aryl, cycloalkyl, and heterocyclyl is optionally substituted with one, two or three substituents selected from R 5 ;  
 
 R 3  and R 3′  are independently selected from: 
 1) H,  
 2) (C═O) a O b C 1 -C 10  alkyl,  
 3) (C═O) a O b aryl,  
 4) (C═O) a O b C 2 -C 10  alkenyl,  
 5) (C═O) a O b C 2 -C 10  alkynyl,  
 6) CO 2 H,  
 7) C 1 -C 6  perfluoroalkyl,  
 8) (C═O) a O b C 3 -C 8  cycloalkyl,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, alkenyl, alkynyl, cycloalkyl, and heterocyclyl is optionally substituted with one, two or three substituents selected from R 5 ;  
 
 or R 3  and R 3′  along with the nitrogen to which they are attached are combined to form ring  
                     
 which is a 5-12 membered nitrogen-containing heterocycle, which is optionally substituted with from one to three R 5  groups and which optionally incoporates from one to two additional heteroatoms, selected from N, O and S in the heterocycle ring;  
 R 4  is independently selected from: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) CO 2 H,  
 4) halo,  
 5) OH,  
 6) O b C 1 -C 6  perfluoroalkyl,  
 7) (C═O) a NR 7 R 8 ,  
 8) CN,  
 9) (C═O) a O b heterocyclyl,  
 10) SO 2 NR 7 R 8 , and  
 11) SO 2 C 1 -C 10  alkyl,  
 said alkyl, aryl, cycloalkyl, and heterocyclyl is optionally substituted with one, two or three substituents selected from R 5 ;  
 
 R 5  is: 
 1) (C═O) a O b C 1 -C 10  alkyl,  
 2) (C═O) a O b aryl,  
 3) C 2 -C 10  alkenyl,  
 4) C 2 -C 10  alkynyl,  
 5) (C═O) a O b  heterocyclyl,  
 6) CO 2 H,  
 7) halo,  
 8) CN,  
 9) OH,  
 10) O b C 1 -C 6  perfluoroalkyl,  
 11) O a (C═O) b NR 7 R 8 ,  
 12) oxo,  
 13) CHO,  
 14) (N═O)R 7 R 8 , or  
 15) (C═O) a O b C 3 -C 8  cycloalkyl,  
 said alkyl, aryl, alkenyl, alkynyl, heterocyclyl, and cycloalkyl optionally substituted with one, two or three substituents selected from R 6 ;  
 
 R 6  is selected from: 
 1) (C═O) r O s (C 1 -C 1  o)alkyl, wherein r and s are independently 0 or 1,  
 2) O r (C 1 -C 3 )perfluoroalkyl, wherein r is 0 or 1,  
 3) oxo,  
 4) OH,  
 5) halo,  
 6) CN,  
 7) (C 2 -C 10 )alkenyl,  
 8) (C 2 -C 10 )alkynyl,  
 9) (C═O) r O s (C 3 -C 6 )cycloalkyl,  
 10) (C═O) r O s (C 0 -C 6 )alkylene-aryl,  
 11) (C═O) r O s (C 0 -C 6 )alkylene-heterocyclyl,  
 12) (C═O) r O s (C 0 -C 6 )alkylene-N(R b ) 2 ,  
 13) C(O)R a ,  
 14) (C 0 -C 6 )alkylene-CO 2 R a ,  
 15) C(O)H,  
 16) (C 0 -C 6 )alkylene-CO 2 H, and  
 17) C(O)N(R b ) 2 ,  
 said alkyl, alkenyl, alkynyl, cycloalkyl, aryl, and heterocyclyl is optionally substituted with up to three substituents selected from R b , OH, (C 1 -C 6 )alkoxy, halogen, CO 2 H, CN, O(C═O)C 1 -C 6  alkyl, oxo, and N(R b ) 2 ;  
 
 R 7  and R 8  are independently selected from: 
 1) H,  
 2) (C═O)O b C 1 -C 10  alkyl,  
 3) (C═O)O b C 3 -C 8  cycloalkyl,  
 4) (C═O)O b aryl,  
 5) (C═O)O b heterocyclyl,  
 6) C 1 -C 10  alkyl,  
 7) aryl,  
 8) C 2 -C 10  alkenyl,  
 9) C 2 -C 10  alkynyl,  
 10) heterocyclyl,  
 11) C 3 -C 8  cycloalkyl,  
 12) SO 2 R a , and  
 13) (C═O)NR b   2 ,  
 said alkyl, cycloalkyl, aryl, heterocylyl, alkenyl, and alkynyl is optionally substituted with one, two or three substituents selected from R 6 , or  
 
 R 7  and R 8  can be taken together with the nitrogen to which they are attached to form a monocyclic or bicyclic heterocycle with 5-7 members in each ring and optionally containing, in addition to the nitrogen, one or two additional heteroatoms selected from N, O and S, said monocylcic or bicyclic heterocycle optionally substituted with one, two or three substituents selected from R 6 ;  
 R a  is (C 1 -C 6 )alkyl, (C 3 -C 6 )cycloalkyl, aryl, or heterocyclyl; and  
 R b  is H, (C 1 -C 6 )alkyl, aryl, heterocyclyl, (C 3 -C 6 )cycloalkyl, (C═O)OC 1 -C 6  alkyl, (C═O)C 1 -C 6  alkyl or S(O) 2 R a .  
 
     
     
         4 . The compound according to  claim 3 , or the pharmaceutically acceptable salt or stereoisomer thereof, wherein R 1  is selected from: (C 1 -C 6 )alkyl, aryl and benzyl, optionally substituted with one or more substituents selected from R 5 .  
     
     
         5 . The compound according to  claim 3 , or the pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2  is selected from: (C 1 -C 6 )alkyl; R 2′  is defined as H; R 1  is selected from: (C 1 -C 6 )alkyl, aryl and benzyl, optionally substituted with one or more substituents selected from R 5 .  
     
     
         6 . A compound which is selected from: 
 N-[1-(3-benzyl-4-oxo-4,5,6,7-tetrahydro-3H-cyclopenta[d]pyrimidin-2-yl)propyl]-4-bromo-N-[2-(dimethylamino)ethyl]benzamide    N-[1-(2-benzyl-1-oxo-1,2,5,6,7,8-hexahydroisoquinolin-3-yl)propyl]-4-bromo-N-[2-(dimethylamino)ethyl]benzamide    or a pharmaceutically acceptable salt or stereoisomer thereof.    
     
     
         7 . A compound selected from:  
       
         
           
                 
               
                     
                 
                     
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                 
                 
                 
                 
                 
               
                   R 1   
                   R 2   
                   R 2′   
                   R 3   
                   R 3′   
                 
                     
                 
                     
                     
                     
                     
                     
                 
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                   Et 
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                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                     
                 
             
                
                
                
                
                
               
            
             
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
               
            
           
         
       
       
         
           
                 
               
                     
                 
                     
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                 
                 
                 
                 
                 
                 
               
                   R 1   
                   R 2   
                   R 2′   
                   R 3   
                   R 3′   
                   (R 4 ) r   
                 
                     
                 
                     
                     
                     
                     
                     
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Cl 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-Me 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-Me 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6,7-dihydroxy 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   7-amino- 6-hydroxy 
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   6-methyl- 7-amino 
                 
                     
                 
                     
                 
             
                
                
                
                
                
               
            
             
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
               
            
           
         
       
       
         
           
                 
               
                     
                 
                     
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                 
                 
                 
                 
               
                     
                     
                     
                     
                 
                   R 1   
                   R 2   
                   R 4   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                     
                     
                     
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   6-Cl 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   6-Cl 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   6-F 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   6-F 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Pr 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   7-F 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   7-Cl 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   7-Cl 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Pr 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   5-F 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   Bn 
                   Et 
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                     
                 
             
                
                
                
                
                
               
            
             
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
               
            
           
         
       
       or a pharmaceutically acceptable salt or stereoisomer thereof.  
     
     
         8 . A pharmaceutical composition that is comprised of a compound in accordance with  claim 1  and a pharmaceutically acceptable carrier.  
     
     
         9 . A method of treating or preventing cancer in a mammal in need of such treatment that is comprised of administering to said mammal a therapeutically effective amount of a compound of  claim 1 .  
     
     
         10 . A method of treating cancer or preventing cancer in accordance with  claim 9  wherein the cancer is selected from cancers of the brain, genitourinary tract, lymphatic system, stomach, larynx and lung.  
     
     
         11 . A method of treating or preventing cancer in accordance with  claim 9  wherein the cancer is selected from histiocytic lymphoma, lung adenocarcinoma, small cell lung cancers, pancreatic cancer, gioblastomas and breast carcinoma.  
     
     
         12 . (canceled)  
     
     
         13 . The composition of  claim 8  further comprising a second compound selected from: 
 1) an estrogen receptor modulator,    2) an androgen receptor modulator,    3) retinoid receptor modulator,    4) a cytotoxic agent,    5) an antiproliferative agent,    6) a prenyl-protein transferase inhibitor,    7) an HMG-CoA reductase inhibitor,    8) an HIV protease inhibitor,    9) a reverse transcriptase inhibitor,    10) an angiogenesis inhibitor, and    11) a PPAR-γ agonist.    
     
     
         14 . (canceled)  
     
     
         15 . (canceled)  
     
     
         16 . A method of treating cancer which comprises administering a therapeutically effective amount of a compound of  claim 1  in combination with radiation therapy.  
     
     
         17 . A method of treating or preventing cancer that comprises administering a therapeutically effective amount of a compound of  claim 1  in combination with a compound selected from: 
 1) an estrogen receptor modulator,    2) an androgen receptor modulator,    3) retinoid receptor modulator,    4) a cytotoxic agent,    5) an antiproliferative agent,    6) a prenyl-protein transferase inhibitor,    7) an HMG-CoA reductase inhibitor,    8) an HIV protease inhibitor,    9) a reverse transcriptase inhibitor, and    10) an angiogenesis inhibitor.    
     
     
         18 . A method of treating cancer that comprises administering a therapeutically effective amount of a compound of  claim 1  in combination with radiation therapy and a compound selected from: 
 1) an estrogen receptor modulator,    2) an androgen receptor modulator,    3) retinoid receptor modulator,    4) a cytotoxic agent,    5) an antiproliferative agent,    6) a prenyl-protein transferase inhibitor,    7) an HMG-CoA reductase inhibitor,    8) an HIV protease inhibitor,    9) a reverse transcriptase inhibitor, and    10) an angiogenesis inhibitor.    
     
     
         19 . A method of treating or preventing cancer which comprises administering a therapeutically effective amount of a compound of  claim 1  and paclitaxel or trastuzumab.  
     
     
         20 . A method of treating or preventing cancer which comprises administering a therapeutically effective amount of a compound of  claim 1  and a GPIIb/IIIa antagonist.  
     
     
         21 . (canceled)  
     
     
         22 . A method of treating or preventing cancer which comprises administering a therapeutically effective amount of a compound of  claim 1  in combination with a COX-2 inhibitor.  
     
     
         23 . A method of modulating mitotic spindle formation which comprises administering a therapeutically effective amount of a compound of  claim 1 .  
     
     
         24 . A method of inhibiting the mitotic kinesin KSP which comprises administering a therapeutically effective amount of a compound of  claim 1.

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