US2004192768A1PendingUtilityA1
Aqueous solution of ascorbic acid and method for producing same
Priority: Nov 30, 2001Filed: Apr 6, 2004Published: Sep 30, 2004
Est. expiryNov 30, 2021(expired)· nominal 20-yr term from priority
Inventors:Dariush Behnam
A23L 33/15A23V 2002/00A61K 31/375A61K 31/355A61K 9/4858A61K 8/4993A61Q 5/00A61K 8/676A61K 31/015A61K 8/0291A23D 7/011A61K 9/1075A61Q 19/00
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Claims
Abstract
Disclosed is an aqueous solution of ascorbic acid which contains an excess of an emulsifier with an HLB value of about 9 to about 18, for example a polysorbate, a method of manufacture of such solution and applications thereof.
Claims
exact text as granted — not AI-modified1 - 18 (cancelled)
19 . Solubilisate consisting of a solution of ascorbic acid in water and a polysorbate, wherein the ascorbic acid part is up to 20% wt and the polysorbate part is about 60% wt to 80% wt and the rest is water, as an addition to aqueous or fatty foodstuff, medicaments and nutrient solutions, cosmetics, fruit juice.
20 . Solubilisate according to claim 1 wherein the weight ratio of ascorbic acid to water amounts to 1:1.
21 . Solubilisate according to claim 1 wherein the utilised polysorbate is polysorbate 80.
22 . Solubilisate according to claim 1 further consisting of an addition of a tocopherol.
23 . Solubilisate according to claim 1 wherein 20% wt of α-tocopherol is mixed with 80% wt polysorbate 20.
24 . Solubilisate according to claim 1 further consisting of an addition of octadecatrienoic acid and/or octadecenoic acid.
25 . Solubilisate according to claim 6 wherein the portion of ascorbic acid within the solution amounts to approximately 5% of wt to approximately 15% wt, and wherein the content of octadecatrienoic acid and/or octadecenoic acid amounts to approximately 10% wt to approximately 20% wt, and the portion of the polysorbate amounts to approximately 60% wt to approximately 75% wt.
26 . Polysorbate according to claim 1 wherein a light oil consisting substantially of triglycerides is added.
27 . Solubilisate according to claim 8 consisting of 10% wt ascorbic acid, 10% wt water, 10% wt of a plant oil an 70% wt polysorbate 80.
28 . Solubilisate according to claim 9 wherein the amount of ascorbic acid and water are reduced to 7% wt, respectively, and the contents of the plant oil and of polysorbate are increased correspondingly.
29 . Solubilisate according to claim 1 wherein the portion of water is decreased to approximately 5% wt to approximately 7% wt and the portion of polysorbate is increased correspondingly.
30 . Solubilisate according to claim 3 consisting of 6.7% wt ascorbic acid, 6.7% wt water, 13.4% wt thistle-oil and 73.2% wt polysorbate.
31 . Method for preparing a solubilisate according to claim 1 wherein up to approximately 20% wt of ascorbic acid are dissolved in water, and wherein approximately 60% wt to approximately 80% wt of a polysorbate is added to the solution, and wherein the mixture is warmed for a short period of time while stirring to clarity and homogeneity.
32 . Method according to claim 13 wherein polysorbate 80 is utilised as a polysorbate.
33 . Method according to claim 13 wherein the mixture is warmed to approximately 80° C.
34 . Method according to claim 13 wherein an oil consisting substantially from triglycerides is added together where the polysorbate to the ascorbic acid solution.
35 . Method according to claim 16 where 70% wt polysorbate together with 10% wt of a light vegetable oil are added to a solution of 10% wt of ascorbic acid in 10% wt water, and wherein the mixture is warmed to at least 60° C. and is stirred to clarity and homogeneity.
36 . Method according to claim 17 wherein the contents of ascorbic acid and of the water each are decreased to approximately 7% wt, and wherein the contents of the vegetable oil and of polysorbate 80 are increased correspondingly.
37 . Method according to claim 13 wherein the portion of water is decreased to approximately 5% wt to approximately 7% wt while the portion of polysorbate is increased correspondingly.
38 . Method according to claim 16 wherein 6.7% wt ascorbic acid is dissolved in the same quantity of water, 13.4% wt of thistle oil being mixed therewith and 73.2% wt of polysorbate are added to the mixture.
39 . Method for preparing a vitamin solubilisate from a solubilisate according to claim 2 having a weight reshow of ascorbic acid to water of 1:1, wherein the solubilisate is stirred with a mixture of 20% wt α-tocopherol and 80% wt polysorbate 20 at a temperature of approximately 50° C.
40 . Method for preparing a vitamin solubilisate from a solubilisate according to claim 2 having a weight reshow of ascorbic acid to water of 1:1, wherein the solubilisate is stirred with a mixture of 10% wt retinol and 90% wt polysorbate 80, the mixture prepared at a temperature of approximately 50° C.
41 . Method for preparing a vitamin solubilisate from a solubilisate according to claim 2 having a weight reshow of ascorbic acid to water 1:1, wherein the solubilisate is mixed with a mixture of 10% wt of a approximately 30% wt β-carotene containing concentrate and 90% wt of polysorbate 80, the mixture being prepared at a temperature of approximately 50° C.
42 . Method for preparing a vitamin solubilisate wherein 85% wt of the solubilisate according to claim 2 having a weight reshow of ascorbic acid to water of 1:1 as mixed with 10% wt of a mixture prepared at 50° C. of 20% wt α-tocopherol and 80% wt polysorbate 20 and with 2% wt of a mixture prepared at approximately 50° C. of 10% wt retinol and 90% wt polysorbate 80 and with 3% wt of a mixture prepared at approximately 50° C. of 10% wt of a 30% β-carotene concentrate with 90% wt polysosrbate 80 in light warmth by stirring.Join the waitlist — get patent alerts
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