US2003234183A1PendingUtilityA1
Movable joint and method for coating movable joints
Assignee: NOBLE MEDICAL COATINGS LLCPriority: May 17, 2001Filed: May 12, 2003Published: Dec 25, 2003
Est. expiryMay 17, 2021(expired)· nominal 20-yr term from priority
A61F 2002/30332A61B 17/00491A61F 2310/00017A61F 2002/3611A61L 27/306A61F 2/30767A61F 2002/3631C25D 5/34A61F 2250/0058A61F 2220/0033A61B 17/86A61F 2002/3625A61F 2002/365A61F 2/30771A61F 2002/30934A61B 17/8665A61F 2310/00449A61F 2/3094A61F 2002/4631C25D 3/04A61F 2/36A61F 2/34A61F 2002/30685A61F 2/32A61F 2310/00029A61F 2002/30535A61F 2/3662
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Claims
Abstract
In a process of electroplating a metal work piece with thin dense chromium, the steps of submerging the metal work piece in a 35% sulfuric acid solution having about 4 ounces per gallon HF as ammonium biflouride salts, and subsequently submerging the metal work piece in a thin dense chromium plating bath having an initial direct current of about 3 volts, the amperages being at about 1.5-2.5 amps per square inch of cathode area, is provided.
Claims
exact text as granted — not AI-modifiedWhat is claimed is:
1 . In a process of electroplating a metal work piece with thin dense chromium, the steps comprising:
a. submerging the metal work piece in a 35% sulfuric acid solution having about 4 ounces per gallon HF as ammonium biflouride salts; and, b. subsequently submerging the metal work piece in a thin dense chromium plating bath having an initial direct current of about 3 volts, the amperages being at about 1.5-2.5 amps per square inch of cathode area.
2 . The process of claim 1 wherein the metal work piece is anodically activated while submerged in said sulfuric acid solution.
3 . The process of claim 2 wherein the anodic activation comprises delivery of about 3 volts direct current for about 30 seconds.
4 . The process of claim 3 wherein about 2-3 amps per square inch of cathode area are provided during anodic activation.
5 . The process of claim 4 wherein said initial direct current voltage is selectively increased over time.
6 . The process of claim 6 wherein said initial direct current voltage is selectively incrementally increased over time.
7 . The process of claim 6 wherein said initial direct current voltage is increased to a maximum of about 4.5 volts.
8 . The process of claim 7 wherein said initial direct current voltage is increased at a rate of 0.1 volt every ten seconds until a voltage of about 4.5 amps is achieved.
9 . A coated implant produced by thin dense chromium plating a work piece, said coated implant having a 100% chromium coating, and a Tabor Abrasion Wear Resistance Wear Index in the range of about 0.9-1.0.
10 . The coated implant of claim 9 wherein said work piece comprises a metal article.
11 . The coated implant of claim 10 wherein said work piece comprises a stainless steel article.
12 . The coated implant of claim 11 wherein said work piece comprises 304 stainless steel.
13 . The coated implant of claim 11 wherein said work piece comprises 401 stainless steel.
14 . The coated implant of claim 10 wherein said work piece comprises a cobalt-chromium article.
15 . The coated implant of claim 10 wherein said work piece comprises a copper article.
16 . The coated implant of claim 10 wherein said work piece comprises an aluminum article.
17 . A coated implant produced by thin dense chrome plating a work piece, said coated implant having a 100% chromium coating, and a Knoop Test microhardness value in excess of 72 HRC.
18 . A coated implant produced by thin dense chromium plating a work piece, said coated implant having a 100% chromium coating and a Vickers Test microhardness value in excess of 67 HRC.
19 . In a process of electroplating a metal work piece with thin dense chromium, the steps comprising:
a. submerging the metal work piece into a thin dense chromium plating solution comprising chromium in the range from about 30 to 35 ounces per gallon of said solution, and sulfuric acid in the range from about 0.3 to 0.35 ounces per gallon of said solution, said solution being at a temperature of about 135-140° Fahrenheit, and carrying a direct current voltage of about 3.2 volts; and, b. upwardly adjusting said direct current voltage at a rate of about 0.1 volt every ten seconds until a direct current voltage of 4.5 is achieved.Join the waitlist — get patent alerts
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